Ch pellets

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This document summarizes different techniques for forming pharmaceutical pellets including agitation, compaction, layering, granulation, and globulation methods. It discusses the spheronization process for pellet formation and describes characterization techniques like tensile strength testing. The document reviews pellet properties like shape and elasticity modulus and provides references on pelletization techniques.

Salud y medicina

Subject: Formulative Pharmacy
BP-502 T
By: Ms. Uditi Handa (Asst. Prof.)
M.Pharma (Ph.D)
GGSCOP, Yamunanagar

IntroductionDefinition:
Pellets Features

Spheronization process
for the pellets formation
1
43
2

Continuing process - Spheronization process for the
pellets formation
5
10
9 8
76

Tensile strength test is used to determine sample behavior under
axial stretching load.
(2014)- the present values of the tensile strength of the pellets in the range from
1.15 MPa to 7.10 Mpa.
(2006)- present values of modulus of elasticity of the pellets in the range from 0.92
Mpa to 1.33 MPa
Characterization of Pellets

References
Preparation of Pellets of Different Shape and Their ...
www.tandfonline.com
Pelletization techniques: A literature review
www.researchgate.net
Pellets and pelletization techniques: A critical review
www.researchgate.net
Pellets and Techniques of Pelletization - RJPT
rjptonline.org ›
pellets and pelletization techniques: a review - ijrpc
www.ijrpc.com
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pellets can be defined as multi particulate system or multiunit system They are spherical particulates manufactured by agglomeration of the powder granules containing drug substance and excipients. Pellets can be prepared by a special technique called Pelletization. This technique is referred to an agglomeration process that convert fine powder or granules of bulk drug or excipient in to small , free flowing , spherical or semi spherical pellets . Multi particular drug delivery system especially suitable for achieving controlled delay released oral formulation with low risk of dose dumping, flexibility of blending to attain different release patterns as well as reproducible and short gastric residence time. Multi particulate drug delivery system are mainly oral dosage form consisting of a multiplicity of small discrete units each exhibiting some desire characteristics.

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PREPARATION AND EVALUATION OF ASPIRIN TABLETS Aim - Preparation and Evaluation of Aspirin Tablets. Requirement – Chemicals - Aspirin, HPMC, PVP, Sodium Stearate, Talc Glasswares - Granulating sieve, standard sieve set, etc. Equipment - Tablet press Principle Aspirin tablet is prepared by wet granulation method. Aspirin belonging to the class of NSAID having analgesic, antipyretic, anti-inflammatory and antiplatelet activity at systematic standard doses. In this Lubricants in combination leads to better drug release kinetic. Aspirin tablets are obtained by wet Compression Method. The particles to be compressed consist of one or more medicaments, with or without excipients substance such as diluents, binders, and disintegration agents, lubricant, glidants. Formula Sr. No. Ingredients Quantity (1 Tab.) 1. Aspirin 250 mg 2. HPMC 50 mg 3. Microcrystalline Cellulose 70 mg 4. Polyvinyl Pyrrolidone Q.S. 5. Sodium Stearate+ Talc 1 mg + 5 mg Method Wet granulation forms the granulation by binding the powders together with an adheshive instead of by compaction. Stages of granule development : A. Pendular B. Funicular C. Capillary D. Droplet Steps involved : Step 1: Weighing and mixing of formulation ingredients. Step 2: Preparing the damp mass. Step 3: Screening the dampened powder into pellets or granules. Step 4: Drying of moist granules. Procedure 1. Tablets were prepared using wet granulation technique as per the composition given earlier. 2. The calculated amount which was required to prepare 400 mg aspirin tablets, containing 250 mg drug, HPMC polymer and PVP as a binder were mixed uniformly. 3. An enough granulating agent (water) was added slowly to prepare wet mass. Granules were prepared by sieving method using a 20# sieve. 4. Further, granules were dried at 35-45ºC for six hours. The dried granules were stored in desiccators until compression of tablets. 5.The required amounts of granules were weighed and compressed using automatically operated tablet punching machine having 12mm flat faced punch diameter and during the tablet preparation to maintain the low resistance between the solid and die wall, lubricants added in granules. Lubricant combinations are agents added in small quantities to the tablet during the tablet preparation. 6. The compressed tablets were stored in airtight container at room temperature for further evaluation. Evaluation 1. Assay : Weigh and powder 20 tablets. Weigh accurately a quantity of the powder containing about 0.5 g of Aspirin, add 30.0 ml of 0.5M sodium hydroxide, boil gently for 10 minutes, cool and titrate the excess of alkali with 0.5 M hydrochloric acid using phenol red solution as indicator. Repeat the operation without the substance under examination. The difference

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Methodology of Preformulation Studies related to Pharmaceutical Sciences. Physio-chemical properties, Program of analytical preformulation. Preformulation Drug Characterization in a Structured Program. Benefits of Preformulation Studies. Bio-pharmaceutical Properties. Bulk Characterization, Solubility analysis, organoleptic properties. Stability studies Pharmaceutical studies objectives of preformulation Need of preformulation studies in Drug Characterization Solubility analysis Dissolution Electrostatic Charges method for Characterization such as UV Spectroscopy, HPLC, TLC, pH determination. Microscopy, Flow Properties Assay development, Lipophilicity pH effect Parentral Preparation Pharmacokinetic Ophthalmic Preparation Isotonicity Suspensions and emulsions Aspirin Pilocarpine penicillin Crystalline compound Amorphous Compound Bioavailability method to determine Partition Coefficient Log P Values Particle Size , Shape and Surface area. Color, taste , odour and physical appearances types of preformulation studies major area of preformulation research absorption metabolism duration of action shake flask method gas chromatography Preformulation Studies: Introduction to preformulation, goals and objectives, study of physicochemical characteristics of drug substances. a. Physical properties: Physical form (crystal & amorphous), particle size, shape, flow properties, solubility profile (pKa, pH, partition coefficient), polymorphism b. Chemical Properties: Hydrolysis, oxidation, reduction, racemisation, polymerization Application of preformulation considerations in the development of solid, liquid oral and parenteral dosage forms and its impact on stability of dosage forms.

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Ch pellets

1. Subject: Formulative Pharmacy BP-502 T By: Ms. Uditi Handa (Asst. Prof.) M.Pharma (Ph.D) GGSCOP, Yamunanagar

2. IntroductionDefinition: Pellets Features

3. 1 2 3 4 NEED!

7. 1. Agitation Method

8. 2. Compactation Method

10. 3. Layering Method

11. 4. Granulation Method

12. 5. Globulation Method

13. 6.

14. Spheronization process for the pellets formation 1 43 2

15. Continuing process - Spheronization process for the pellets formation 5 10 9 8 76

16. Tensile strength test is used to determine sample behavior under axial stretching load. (2014)- the present values of the tensile strength of the pellets in the range from 1.15 MPa to 7.10 Mpa. (2006)- present values of modulus of elasticity of the pellets in the range from 0.92 Mpa to 1.33 MPa Characterization of Pellets

17. Marketed Products

18. References Preparation of Pellets of Different Shape and Their ... www.tandfonline.com Pelletization techniques: A literature review www.researchgate.net Pellets and pelletization techniques: A critical review www.researchgate.net Pellets and Techniques of Pelletization - RJPT rjptonline.org › pellets and pelletization techniques: a review - ijrpc www.ijrpc.com Thank You

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